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Extractive Distillation

Extractive Distillation

3 days
PSE/DISTEXT-E
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Sessions
Who should attend?
Learning Objectives
Course Content
Ways & Means
Sessions
This course is not scheduled.
Who should attend?

Audience

    • Anyone involved in the operation of extractive distillation columns (engineers, shift leaders, panel operators, field operators).

Level

  • Proficiency
  • This course provides a deeper technical understanding of an extractive distillation column and its principle.
Learning Objectives
  • Upon completion of the course, the participants will be able to:
  • know about the action of the solvent,
  • explain the significance of operating parameters,
  • analyze the effect of each parameter acting on the operation of the column and on the qualities of products,
  • counteract the most frequent incidents.
Course Content

SOLVENT EFFECT ON LIQUID-VAPOR EQUILIBRIA

0.75 day
  • Typical composition of cuts to be treated: C4 and C6 cuts of a steamcracker or other units.
  • Natural volatility of compounds and focus on impurities to be removed, highlighting constraints and treatments available.
  • Action of the solvent and effects on relative volatilities of compounds for separation.
  • Effects of pressure, solvent ratio and feed composition.

BEHAVIOR OF AN EXTRACTIVE DISTILLATION COLUMN

0.75 day
  • Feed composition. Qualities required.
  • Mass balance, product recovery ratio, losses of solvent.
  • Analysis of operating parameters: pressure and its control system, solvent ratio, solvent temperature, thermal balance and liquid-vapor traffics.
  • Concentration profile: HC and solvent, behaviors in extractive and non-extractive zones.
  • Meaning of temperatures and of its profile.

DOWNSTREAM TREATMENT

0.5 day
  • Solvent recovery system and purification.
  • Make-up of solvent and adjustment of its composition in the solvent loop.
  • Superfractionation if needed.

OPERATING VARIABLES OF AN EXTRACTIVE DISTILLATION COLUMN

0.5 day
  • Instrumentation and process control scheme.
  • Meaning of tuned parameters.
  • Modification impact of: solvent ratio, reboiler ratio, solvent temperature and other parameters depending on the process configuration.

UPSETS & INCIDENTS

0.5 day
  • Solvent: decrease in flowrate, temperature modification, regeneration trouble and loss of recycling.
  • Feed: unexpected change in flowrate or composition.
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Upstream Budget Practice

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Upstream Contracts Audit

Upstream Contracts Audit

Upstream Auditing Certification

Upstream Auditing Certification

Governance of an E&P Company

Governance of an E&P Company

Ways & Means
  • Implementation of static simulation results with C4/ACN and C6/NMP treatment.
  • Working groups to study operating situations that could arise.

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