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  4. Operation of a Binary Distillation Column - Level 2
Operation of a Binary Distillation Column - Level 2

Operation of a Binary Distillation Column - Level 2

5 days
PSE/CCDSS-E
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Sessions
Who should attend?
Learning Objectives
Course Content
Ways & Means
Sessions
This course is not scheduled.
Who should attend?

Audience

    • Console operators and production supervisors, shift supervisors.

Level

  • Proficiency
  • This course provides a deeper understanding of operating distillation columns under all conditions, with a practical understanding of operations and control systems through a hands-on experience.
Learning Objectives
  • Upon completion of the course, the participants will be able to:
  • achieve normal column operation with common control strategies,
  • be familiar with all parameters and profiles for the analysis of distillation columns,
  • understand the concepts necessary for optimizing the column on the basis of typical economics and constraints,
  • anticipate, recognize and react to disturbances in order to maintain safe operation and avoid negative economic consequences,
  • be thoroughly familiar with the main steps of start-up and shutdown procedures.
Course Content

OPERATING PARAMETERS

1 day
  • Behavior of flash mixtures: vaporized fraction, liquid-vapor separation and distribution of components according to their volatility.
  • Material balance of the column: concepts of cut point, separation quality and fractionation capability.
  • Heat balance: reflux and reboiling ratios and selectivity assessment.
  • Column pressure effects: pressure control and pressure profile along the column - Flow rates, concentration and temperature profiles.

FRACTIONATION CAPABILITY

0.5 day
  • The trainees will experience these causes and effects on a debutanizer simulator.
  • Effects of liquid-vapor flow rates, reflux and reboiling ratios on separation - Influence of liquid-vapor traffic on concentration and temperature profiles.
  • Separation quality and its relationship to energy consumption.

MASS BALANCE & IMPLEMENTATION OF A TEMPERATURE CONTROL

0.5 day
  • Impact of reflux and reboiler duty on material balance, and consequences on product specifications.
  • Impact of disturbances on column mass balance and product purities.
  • Definition of, and how to identify the Sensitive tray, and its influence on concentration profiles and products qualities.
  • Implementation of sensitive temperature control systems, advantages and limitations.

OTHER PROCESS CONTROL PARAMETERS

1.5 days
  • Survey of operating disturbances, their common origins and causes - Pressure control and its impact on column stability.
  • Analysis of disturbances caused by the feed, composition, temperature or flow rate.
  • Reboiler fouling, loss of condensing, and tray flooding - External and internal reflux control, and reboiling control by means of flowrates or duty.
  • Optimizing heat balance, influence of additional energy through feed or reboiler, and benefits of low pressure operation.
  • Implementation of control systems based on quality measurement.

UPSETS

1 day
  • Operation of the column at its limits: thermal equipment fouling, cooling water troubles and flooding - Failures of instruments and pumps.

START-UP - SHUTDOWN

0.5 day
  • Analysis of the behavior in the column at each step of start-up and shutdown.

SIMULATOR TRAINING

  • Exercises are conducted in small groups of 2 to 3 participants, each group operating its own virtual column. Each exercise includes: a pre-discussion of the problem; definition of the target exercise objective; adequate time to run the virtual columns; open analysis of the results, shared with all participants; and practical conclusions related to the operation of the columns.
  • Attendees are invited to bring descriptions of their specific column control strategies for group discussion and analysis. Conclusions drawn from the exercises on the simulator can be transposed to other actual control schemes.
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E-595C - Maintenance Management Certification

E-595C - Maintenance Management Certification

E-595C - Maintenance Management Certification

E-597 - Corrosion Prevention in Production Facilities

E-597 - Corrosion Prevention in Production Facilities

E-597 - Corrosion Prevention in Production Facilities

E-597 - Corrosion Prevention in Production Facilities

E-599 - Subsea Integrity Management (I) - Inspection, Monitoring & Testing

E-599 - Subsea Integrity Management (I) - Inspection, Monitoring & Testing

E-599 - Subsea Integrity Management (I) - Inspection, Monitoring & Testing

E-599 - Subsea Integrity Management (I) - Inspection, Monitoring & Testing

E-600 - Subsea Integrity Management (II) - Non Conformity Management

E-600 - Subsea Integrity Management (II) - Non Conformity Management

E-600 - Subsea Integrity Management (II) - Non Conformity Management

E-600 - Subsea Integrity Management (II) - Non Conformity Management

E-601C - HSE Engineer Certification

E-601C - HSE Engineer Certification

E-601C - HSE Engineer Certification

E-601C - HSE Engineer Certification

E-606 - Environmental & Social Risk Management

E-606 - Environmental & Social Risk Management

E-606 - Environmental & Social Risk Management

E-606 - Environmental & Social Risk Management

E-607 - Social Risk Management

E-607 - Social Risk Management

E-607 - Social Risk Management

E-607 - Social Risk Management

E-608 - Environmental Management

E-608 - Environmental Management

E-608 - Environmental Management

E-608 - Environmental Management

E-614 - Environmental Pollution & Waste Management

E-614 - Environmental Pollution & Waste Management

E-614 - Environmental Pollution & Waste Management

E-614 - Environmental Pollution & Waste Management

E-620C - Safety Engineering Certification

E-620C - Safety Engineering Certification

E-620C - Safety Engineering Certification

E-620C - Safety Engineering Certification

E-622 - Safety Engineering - Module 1

E-622 - Safety Engineering - Module 1

E-622 - Safety Engineering - Module 1

E-622 - Safety Engineering - Module 1

E-624 - Safety Engineering - Module 2

E-624 - Safety Engineering - Module 2

E-624 - Safety Engineering - Module 2

E-624 - Safety Engineering - Module 2

E-626 - Safety Engineering - Module 3 (Project)

E-626 - Safety Engineering - Module 3 (Project)

E-626 - Safety Engineering - Module 3 (Project)

E-626 - Safety Engineering - Module 3 (Project)

E-630C - NEBOSH International Certificate in Oil & Gas Operational Safety

E-630C - NEBOSH International Certificate in Oil & Gas Operational Safety

E-630C - NEBOSH International Certificate in Oil & Gas Operational Safety

E-630C - NEBOSH International Certificate in Oil & Gas Operational Safety

E-643 - HSE in Laboratory

E-643 - HSE in Laboratory

E-648 - Construction HSE Management

E-648 - Construction HSE Management

E-648 - Construction HSE Management

E-648 - Construction HSE Management

E-700 - Engineering of Upstream Projects

E-700 - Engineering of Upstream Projects

E-702 - Technical Standards for Surface Facilities Design

E-702 - Technical Standards for Surface Facilities Design

E-702 - Technical Standards for Surface Facilities Design

E-702 - Technical Standards for Surface Facilities Design

E-712 - E&P Value Chain & Front-End Development

E-712 - E&P Value Chain & Front-End Development

E-712 - E&P Value Chain & Front-End Development

E-712 - E&P Value Chain & Front-End Development

E-714 - Offshore E&P Project Management

E-714 - Offshore E&P Project Management

E-714 - Offshore E&P Project Management

E-714 - Offshore E&P Project Management

E-715C - E&P Logistics Engineer Certification

E-715C - E&P Logistics Engineer Certification

E-716 - E&P Project Logistics Management

E-716 - E&P Project Logistics Management

E-716 - E&P Project Logistics Management

E-716 - E&P Project Logistics Management

E-710C - E&P Project Management Certification

E-710C - E&P Project Management Certification

E-710C - E&P Project Management Certification

E-710C - E&P Project Management Certification

E-720C - Project Control Certification

E-720C - Project Control Certification

E-721 - E&P Project Control Tools

E-721 - E&P Project Control Tools

E-721 - E&P Project Control Tools

E-721 - E&P Project Control Tools

E-722 - E&P Technical Service Contracts

E-722 - E&P Technical Service Contracts

E-722 - E&P Technical Service Contracts

E-722 - E&P Technical Service Contracts

E-723 - E&P Technical Contract Negotiation

E-723 - E&P Technical Contract Negotiation

E-723 - E&P Technical Contract Negotiation

E-723 - E&P Technical Contract Negotiation

E-725 - E&P Project Operating Expenses Optimization

E-725 - E&P Project Operating Expenses Optimization

E-725 - E&P Project Operating Expenses Optimization

E-725 - E&P Project Operating Expenses Optimization

E-724C - E&P Project Cost Estimation & Control Certification

E-724C - E&P Project Cost Estimation & Control Certification

E-724C - E&P Project Cost Estimation & Control Certification

E-724C - E&P Project Cost Estimation & Control Certification

E-730 - Upstream Project Construction Management Training

E-730 - Upstream Project Construction Management Training

E-732 - Upstream Project Construction Site Administration

E-732 - Upstream Project Construction Site Administration

E-732 - Upstream Project Construction Site Administration

E-732 - Upstream Project Construction Site Administration

E-733 - Upstream Project Construction HSE Management

E-733 - Upstream Project Construction HSE Management

E-733 - Upstream Project Construction HSE Management

E-733 - Upstream Project Construction HSE Management

E-734 - Offshore Oil & Gas Project Installation

E-734 - Offshore Oil & Gas Project Installation

E-734 - Offshore Oil & Gas Project Installation

E-734 - Offshore Oil & Gas Project Installation

E-736 - Upstream Project Precommissioning, Commissioning & Start-Up

E-736 - Upstream Project Precommissioning, Commissioning & Start-Up

E-736 - Upstream Project Precommissioning, Commissioning & Start-Up

E-736 - Upstream Project Precommissioning, Commissioning & Start-Up

E-737 - Upstream Project Abandonment Operations

E-737 - Upstream Project Abandonment Operations

E-737 - Upstream Project Abandonment Operations

E-737 - Upstream Project Abandonment Operations

E-739C - Construction Superintendent Certification

E-739C - Construction Superintendent Certification

E-739C - Construction Superintendent Certification

E-739C - Construction Superintendent Certification

Recent Developments in Oil Refining Technologies

Recent Developments in Oil Refining Technologies

Air Separation Unit

Air Separation Unit

Applied Chemical Engineering Certification

Applied Chemical Engineering Certification

Select Thermodynamic Models for Simulation

Select Thermodynamic Models for Simulation

Troubleshooting in the Oil & Gas Industry

Troubleshooting in the Oil & Gas Industry

Troubleshooting in the Oil & Gas Industry

Troubleshooting in the Oil & Gas Industry

Chemical Reaction Engineering

Chemical Reaction Engineering

Reactor Engineering

Reactor Engineering

Distillation Certification

Distillation Certification

Operation of a Binary Distillation Column - Level 1

Operation of a Binary Distillation Column - Level 1

Operation of a Binary Distillation Column - Level 2

Operation of a Binary Distillation Column - Level 2

Operation of a Multiple-Draw Distillation Column

Operation of a Multiple-Draw Distillation Column

Distillation Column Internals

Distillation Column Internals

Catalysts in Refining Processes

Catalysts in Refining Processes

Hydrotreatment Processes

Hydrotreatment Processes

Hydrotreatment Processes

Hydrotreatment Processes

Crude Oil & Vacuum Distillation

Crude Oil & Vacuum Distillation

Catalytic Reforming for Refining & Petrochemicals

Catalytic Reforming for Refining & Petrochemicals

Isomerization

Isomerization

Fluid Catalytic Cracking Operation

Fluid Catalytic Cracking Operation

Alkylation (HF or H<sub>2</sub>SO<sub>4</sub>)

Alkylation (HF or H2SO4)

Hydrocracking

Hydrocracking

Hydrogen Production Unit

Hydrogen Production Unit

Gas Purification with PSA

Gas Purification with PSA

H<sub>2</sub>S Removal & Sulfur Recovery Processes

H2S Removal & Sulfur Recovery Processes

Visbreaking

Visbreaking

Cokefaction

Cokefaction

Extra Heavy Crude Oil Upgrading

Extra Heavy Crude Oil Upgrading

Cracked Gases Separation

Cracked Gases Separation

Cracking & Chemical Treatments of Purification

Cracking & Chemical Treatments of Purification

Selective Hydrogenation of the Steamcracker

Selective Hydrogenation of the Steamcracker

Production of Paraxylene - Aromatic Loops

Production of Paraxylene - Aromatic Loops

Extractive Distillation

Extractive Distillation

Ether Production MTBE or ETBE

Ether Production MTBE or ETBE

Base Chemicals & Polymers Manufacturing*

Base Chemicals & Polymers Manufacturing*

Polymer Reaction Engineering

Polymer Reaction Engineering

Rheology - Polymers Characterization

Rheology - Polymers Characterization

Main Polymers PE/PP/PS

Main Polymers PE/PP/PS

Ethylene Compression & Hypercompressors for LDPE Units

Ethylene Compression & Hypercompressors for LDPE Units

Chlorine & PVC Value Chain

Chlorine & PVC Value Chain

Production of Synthetic Elastomers

Production of Synthetic Elastomers

Extrusion & Pelletizing Polymers

Extrusion & Pelletizing Polymers

Compounding Polymers Processes

Compounding Polymers Processes

Acrylic Acid & Lights Acrylates Units

Acrylic Acid & Lights Acrylates Units

Petroleum Products

Petroleum Products

Current & Future Automotive Fuels

Current & Future Automotive Fuels

Storage of Petroleum Products: Storage Equipment & Tank Operation

Storage of Petroleum Products: Storage Equipment & Tank Operation

Properties, Formulation, Transfer & Storage of Petroleum Products

Properties, Formulation, Transfer & Storage of Petroleum Products

Automation of Refinery Offsite Operations

Automation of Refinery Offsite Operations

Recent Developments & Innovation in Equipment

Recent Developments & Innovation in Equipment

Static Equipment

Static Equipment

Corrosion & Corrosion Prevention Certification

Corrosion & Corrosion Prevention Certification

Painting & Coating for Corrosion Resistance

Painting & Coating for Corrosion Resistance

Inspector Certification

Inspector Certification

Process Energy Efficiency Improvement for Industrial Plants

Process Energy Efficiency Improvement for Industrial Plants

Day-to-Day Energy Optimization for Industrial Plants

Day-to-Day Energy Optimization for Industrial Plants

Heat Exchangers Certification

Heat Exchangers Certification

Furnaces: Safe Operation & Optimization

Furnaces: Safe Operation & Optimization

Tubular Furnaces

Tubular Furnaces

Boilers Safe Operation & Optimization

Boilers Safe Operation & Optimization

Refrigeration Unit Operation

Refrigeration Unit Operation

Gas Compression & Expansion: Compressors & Turbines Certification

Gas Compression & Expansion: Compressors & Turbines Certification

Gas Turbines Certification

Gas Turbines Certification

Centrifugal Pumps & Positive Displacement Pumps

Centrifugal Pumps & Positive Displacement Pumps

Reciprocating Compressors

Reciprocating Compressors

Centrifugal Compressors

Centrifugal Compressors

Steam Turbines

Steam Turbines

Machinery Failure Analysis & Repair Methods

Machinery Failure Analysis & Repair Methods

Machinery Vibration

Machinery Vibration

Rotating Machinery: Troubleshooting Analysis

Rotating Machinery: Troubleshooting Analysis

Instrumentation & Process Control Certification

Instrumentation & Process Control Certification

Advanced Process Control

Advanced Process Control

Multivariable Predictive Control

Multivariable Predictive Control

Design & Operation of a Safety Instrumented System (SIS)

Design & Operation of a Safety Instrumented System (SIS)

Electrical Motors: Technology, Operation & Maintenance

Electrical Motors: Technology, Operation & Maintenance

Maintenance Management & Equipment Availability Certification

Maintenance Management & Equipment Availability Certification

Routine Maintenance Optimization

Routine Maintenance Optimization

Turnaround Management

Turnaround Management

Mentors Training Course

Mentors Training Course

Train The Trainers

Train The Trainers

Safety in Operation Related to Chemical & Oil Storage

Safety in Operation Related to Chemical & Oil Storage

Waste Water Treatment

Waste Water Treatment

Improve Your SHE Management System

Improve Your SHE Management System

Industrial Safety Engineer Certification

Industrial Safety Engineer Certification

Management of Site Projects Certification

Management of Site Projects Certification

Engineering Contracts

Engineering Contracts

Processes Representation

Processes Representation

Processes Representation

Processes Representation

Electric Drives for Automotive Propulsion Design, Modeling & Simulation

Electric Drives for Automotive Propulsion Design, Modeling & Simulation

IC Engine Training for Engineers

IC Engine Training for Engineers

Engine Design

Engine Design

Engine Reliability

Engine Reliability

Engine Cooling & Environment

Engine Cooling & Environment

Powertrain NVH

Powertrain NVH

Engine Parts Design

Engine Parts Design

New Combustion Systems in Spark Ignited Engines

New Combustion Systems in Spark Ignited Engines

New Combustion Developments in Diesel Engines

New Combustion Developments in Diesel Engines

Exhaust Gas After-Treatment

Exhaust Gas After-Treatment

Loading & Supercharging

Loading & Supercharging

Advanced Loading and Supercharging Modelings, Simulations and Analyses

Advanced Loading and Supercharging Modelings, Simulations and Analyses

Engine Measurements and Calibrations

Engine Measurements and Calibrations

Engine Measurements Tests Analysis & Calibrations

Engine Measurements Tests Analysis & Calibrations

Diesel Engines Performances - Level 1

Diesel Engines Performances - Level 1

Diesel Engines Performances - Level 2

Diesel Engines Performances - Level 2

Engine Management: Control Software & Calibration

Engine Management: Control Software & Calibration

Engine Calibration & Tuning

Engine Calibration & Tuning

Gasoline Engine Management

Gasoline Engine Management

Diesel Engine Management

Diesel Engine Management

Introduction to Engine Management: Practical Approach by Modeling & Simulation

Introduction to Engine Management: Practical Approach by Modeling & Simulation

Engine Management Training

Engine Management Training

Lubrication & Lubricants

Lubrication & Lubricants

Car Engines Lubrication

Car Engines Lubrication

Industrial Engines Lubrication & Technology

Industrial Engines Lubrication & Technology

Lubrication & Technology of Automotive Transmissions

Lubrication & Technology of Automotive Transmissions

Lubricating Greases Automotive & Industrial Applications

Lubricating Greases Automotive & Industrial Applications

Lubrication & Technology of Industrial Equipment

Lubrication & Technology of Industrial Equipment

Lubrication of Metal Working Operations & Machine Tools

Lubrication of Metal Working Operations & Machine Tools

Powertrain Functional Safety

Powertrain Functional Safety

Vehicle Fuel Consumption

Vehicle Fuel Consumption

Vehicle Performances

Vehicle Performances

Vehicle Emissions

Vehicle Emissions

Drivability

Drivability

0D Powertrain Modeling

0D Powertrain Modeling

1D Powertrain Modeling

1D Powertrain Modeling

3D Powertrain Modeling

3D Powertrain Modeling

PROMISE™ - Oil & Gas Project Management Interactive Simulator for Excellence

PROMISE™ - Oil & Gas Project Management Interactive Simulator for Excellence

E&P Companies in Changing Environment

E&P Companies in Changing Environment

Production Sharing & Joint Operating Agreements

Production Sharing & Joint Operating Agreements

Dispute Resolution in the Upstream Activity

Dispute Resolution in the Upstream Activity

Negotiation of Exploration-Production Contracts

Negotiation of Exploration-Production Contracts

Operating under

Operating under "Local Content"

Oil Fields Unitization

Oil Fields Unitization

Practice of Exploration-Production Contracts Economic Modeling

Practice of Exploration-Production Contracts Economic Modeling

Economics & Risk Analysis of Upstream Projects

Economics & Risk Analysis of Upstream Projects

Upstream Economist Certification

Upstream Economist Certification

Upstream Module

Upstream Module

Oil Markets & Trading

Oil Markets & Trading

Price Risk Management in Energy Markets

Price Risk Management in Energy Markets

Shipping: General Features, Chartering Contracts & Operations

Shipping: General Features, Chartering Contracts & Operations

Planning & Economics of Refinery Operations

Planning & Economics of Refinery Operations

Refinery Operation Management & Linear Programming

Refinery Operation Management & Linear Programming

Economic Optimization of Refining Operations

Economic Optimization of Refining Operations

Refining & Petrochemicals Synergies

Refining & Petrochemicals Synergies

Profitability Analysis of Downstream Investment Projects

Profitability Analysis of Downstream Investment Projects

Downstream Module

Downstream Module

Marketing & Sales of Lubricants

Marketing & Sales of Lubricants

Supply Chain Management

Supply Chain Management

Gas Markets & Trading

Gas Markets & Trading

Contractual Framework of Gas Sale-Purchase & Transportation

Contractual Framework of Gas Sale-Purchase & Transportation

Legal Issues Relating to FSRU Projects

Legal Issues Relating to FSRU Projects

Negotiating LNG Master Sale & Purchase Agreement

Negotiating LNG Master Sale & Purchase Agreement

Natural Gas & Electricity Trading

Natural Gas & Electricity Trading

Econometrics & Forecasting

Econometrics & Forecasting

Assess Energy Efficiency & CO<sub>2</sub> Reduction

Assess Energy Efficiency & CO2 Reduction

Financial Management of an International Oil & Gas Company

Financial Management of an International Oil & Gas Company

Upstream Budget Practice

Upstream Budget Practice

Upstream Contracts Audit

Upstream Contracts Audit

Upstream Auditing Certification

Upstream Auditing Certification

Governance of an E&P Company

Governance of an E&P Company

Ways & Means
  • Use of a virtual column modeled on RSI IndissPlus dynamic simulators.

Legal Information

General Terms of Sale

Personal Data Protection

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